Comparison of properties of bituminous binders after aging by different methods

published:
Number: Issue 26(2022)
Section: Construction and civil engineering
The page spacing of the article: 92–107
Keywords: adhesion, paving bitumen, methods ageing, penetration, softening point temperature
How to quote an article: Yan Pyrig, Andrii Galkin, Serhii Oksak. Comparison of properties of bituminous binders after aging by different methods. Dorogi і mosti [Roads and bridges]. Kyiv, 2022. Iss. 26. P. 92–107 [in Ukrainian].

Authors

Kharkiv National Automobile and Highway University, Kharkiv, Ukraine
https://orcid.org/0000-0002-1904-5618
Kharkiv National Automobile and Highway University (KNAHU), Kharkiv, Ukraine
https://orcid.org/0000-0002-3084-3469
Kharkiv National Automobile and Highway University (KNAHU), Kharkiv, Ukraine
https://orcid.org/0000-0003-0957-2251

Summary

Introduction. The performance and durability of asphalt pavements are majorly conditioned by the quality of the bituminous binders. One of the main disadvantages of asphalt pavements is the permanent change in their properties in time due to the aging of the binder. Various laboratory methods of aging are used to predict the intensity of changes in the properties of bituminous binders that occur during the asphalt mixing at plants and the lifetime of asphalt concrete in the pavement.

Problem Statement. In Ukraine, with the implementation of European principles of standardization and the transition to harmonized European standards, there is a gradual replacement of the aging method ГОСТ 18180, which has long been used in the domestic road industry, with the world-accepted RTFOT aging method. Due to the different conditions set in these methods of aging, the question of the impact of differences in aging regimes on the properties of bituminous binders, the possibility of comparing the results obtained by these two methods and the interchangeability of methods is topical.

Purpose. The aim of the work is to obtain the influence of the methods of aging adopted in the road industry of Ukraine on the change of properties of road viscous bitumens and bituminous binders, modified with various additives.

Materials and methods. Viscous bitumens and bituminous binders modified with various additives (adhesive additives, polymers, structuring additives) used in the domestic road industry are used as objects of research. For methods of aging the domestic method ГОСТ 18180 (for a long time this method was the only one in Ukraine used for estimation of change of properties of bituminous binders under the influence of technological temperatures and which, under test conditions, is close to the standardized method TFOT), as well as the world’s widespread RTFOT method of aging are used.

Results. Based on the obtained experimental data, it is found that aging by the ГОСТ 18180 method has a slightly greater effect on the change of properties than after aging by the RTFOT method. The least sensitive indicator of aging conditions is the breaking point temperature — the difference between the values of this indicator after aging by different methods is within the convergence of the method. The conditions of the aging method have the greatest effect on the quality of bitumens modified with adhesives. The relatively short heating time of binders in accordance with the conditions of the RTFOT aging method leads to less change in the adhesion of binders to the glass surface, which may contribute to misleading in thermal stability of adhesives.

Conclusions. When revising the domestic standards for technical conditions for bituminous binders, which provide for the replacement of the aging method according to GOST 18180 by the RTFOT method and setting of limits for changing the standard quality of binders after aging, should take into account the slightly lower aging intensity of RTFOT binders. This is especially true for the adhesion requirements of bitumens modified with adhesives.

 

References

  1. Kolbanovskaja A.S., Mihajlov V.V. Dorozhnye bitumy [Road bitumen]. Мoscow, 1973. 264 p. [in Russian].
  2. Bell C.A. Summary report on aging of asphalt-aggregate systems. Strategic Highway Research Program, National Research Council, 1989. Т. 89. №. 4. 121 р. [in English].
  3. Richardson C. The modern asphalt pavement. New York – London. J. Wiley & Sons, 1907. 652 p. [in English].
  4. Lewis R.H., Welborn J.Y. The Properties of the Residues of 50-60 and 85-100 Penetration Asphalts from Oven Tests and Exposure. Public Roads. 1941. № 22. Р. 27–49 [in English].
  5. Lee D.Y. Durability and Durability Tests for Paving Asphalt: A State of the Art Report. Engineering Research Institute, Iowa State University, 1969. 50 p. [in English].
  6. Airey G.D. State of the art report on ageing test methods for bituminous pavement materials. International Journal of Pavement Engineering. 2003, Т.4, №. 3. P. 165–176 [in English].
  7. Welborn J.Y. Physical properties as related to asphalt durability: State of the art. Transportation Research Record, 1984.  №. 999. Р. 31–36 [in English].
  8. Davison R.R. et al. Development of Gel Permeation Chromatography, Infrared and Other Tests to Characterize Asphalt Cements and Correlate with Field Performance. Volume I. Austin, Texas. 1989. 274 р. [in English].
  9. Speight J.G. Asphalt materials science and technology. Butterworth-Heinemann, Oxford, UK. 2016. 631 р. [in English].
  10. Finn F.N., Yapp M.T., Coplantz J.S., Durrani A.Z. Asphalt properties and relationship to pavement performance. Literature Review. Scotts Valley, California. 1990. 404 р. [in English].
  11. Słowik M., Adamczak P. Evaluation of short-term ageing influence on the properties of SBS elastomer modified road bitumens. Roads and Bridges. Drogi i Mosty. 2007. Т. 6. №.1. Р. 41–58 [in English].
  12. Lu X., Isacsson U. Effect of ageing on bitumen chemistry and rheology. Construction and Building materials. 2002. Т. 16. №. 1. Р. 15–22 [in English].
  13. Button J.W., Little D.N., Gallaway B.M., Epps J.A. Influence of asphalt temperature susceptibility on pavement construction and performance. NCHRP Report. 1983. №. 268. 72 р. [in English].
  14. Glover C.J., Davison R.R., Vassiliev N., Hausman T., Williamson S. A. Development of stirred air-flow test (SAFT) for improved HMAC plant binder aging simulation and studies of asphalt air blowing. Texas Transportation Institute. 2001. 80 р. [in English].
  15. Shiau J.M., Tia M., Ruth B.E., Page C.G. Evaluation of aging characteristics of asphalts by using TFOT and RTFOT at different temperature levels. Transportation Research Record. 1992. №. 1342. Р. 58–66 [in English].
  16. Phromsorn C. J., Kennedy T.W. Evaluation of laboratory methods simulating aging effects of asphalt binder. Transportation research record. № 1488. 1995. Р. 13–20 [in English].
  17. Starickij M.G. Metody ispytanija bitumnyh i degtevyh dorozhno-stroitel’nyh materialov [Methods for testing bitumen and tar road building materials]. M.: Dorizdat GUShOSDORA NKVD SSSR, 1941. 216 p. [in Russian].
  18. Shiperovich V.L. Neftjanye bitumy i ih primenenie v dorozhnom dele [Petroleum bitumens and their use in road construction]. M.: Neftesindikat, 1929. 40 p. [in Russian].
  19. Metcger G. Issledovanie svojstv dorozhnyh bituminoznyh materialov SSSR [Research of properties of road bituminous materials of the USSR]. Leningrad: Gosudarstvennoe transportnoe izdatel’stvo, 1935. 74 p. [in Russian].
  20. HOST 2400-51. Bitumy neftjanye. Metody ispytanij [Oil bitumen. Test Methods]. Moskva: Upravlenie po standartizacii pri Sovete Ministrov SSSR. 1952. 5 p. [in Russian].
  21. HOST 18180-72 (ST SJeV 4543-84) Bitumy neftjanye. Metod opredelenija izmenenija massy posle progreva [State  Standard of  Ukraine (HOST 18180-72) Petroleum bitumens. Method for determination of mass change after heating]. Мoscow. 1972. 4 p. (Information and documentation) [in Russian].
  22. Besamusca J., Sorensen A., Southwell С. Addressing ageing characteristics of bituminous binders in Europe. Eurasphalt & Eurobitume Congress, 5th, 2012, Istanbul, Turkey. 2012.  Р. 1–11 [in English].
  23. DSTU B EN 12607-1:2015 (EN 12607-1:2014, IDT) Bіtum ta bіtumnі vyazhuchі. Viznachennja oporu do tverdіnnja pіd vplivom teploti ta povіtrja. Chastina 1. Metod RTFOT. [State Standard of Ukraine (DSTU B EN 12607-1:2015 (EN 12607-1:2014, IDT)) Bitumen and bituminous binders – Determination of the resistance to hardening under influence of heat and air. Part 1: RTFOT method]. Kyiv, 2016. 23 p. (Information and documentation) [in Ukrainian].
  24. DSTU EN 12607-2:2019 (EN 12607-2:2014, IDT) Bіtum ta bіtumnі vyazhuchі. Viznachennja oporu do tverdіnnja pіd vplivom tepla ta povіtrja. Chastina 2. Metod TFOT. [State Standard of Ukraine (DSTU EN 12607-2:2019 (EN 12607-2:2014, IDT)) Bitumen and bituminous binders - Determination of the resistance to hardening under influence of heat and air - Part 2: TFOT Method]. Kyiv, 2019. 20 p. (Information and documentation) [in Ukrainian].
  25. Kopynets І. Resilience of oxidized bіtumen to thermal-oxidative. Dorogi і mosti [Roads and bridges]. Kyiv, 2014. 14. P. 14–20 [in Ukrainian].
  26. Kіshhinskii S.V., Kopynets І.V. Pіdvishhennja stіjkostі okislenih bіtumіv do starіnnja shljahom їh kompaunduvannja z distiljacіjnimi bіtumami [Advancement of the resistance of oxidized bitumens to antiquity by means of compounding with distillation bitumens]. Avtoshljahovik Ukraїni. 2015. №. 5. P. 50–52 [in Ukrainian].
  27. Zolotarev V.A., Kopinec I.V. Sravnitelnoye issledovanie okislennyh i ostatochnyh bitumov v staticheskom i dinamicheskom rezhimah starenija [Comparative study of oxidized and residual bitumen in static and dynamic aging modes]. Dorogi i mosty. 2017. № 35/1. P. 215–232 [in Russian].
  28. DSTU EN 12593:2018 (EN 12593:2015, IDT) Bіtum ta bіtumnі vyazhuchі. Viznachennja temperaturi krihkostі za metodom Fraasa. [State Standard of Ukraine (DSTU EN 12593:2018 (EN 12593:2015, IDT)) Bitumen and bituminous binders - Determination of the Fraass breaking point]. Kyiv, 2019. 18 p. (Information and documentation) [in Ukrainian].
  29. DSTU EN 1427 (EN 1427:2015, IDT) Bіtum ta bіtumnі vyazhuchі. Viznachennja temperaturi rozmyakshenostі za metodom kіltsa і kulі. [State Standard of Ukraine (DSTU EN 1427 (EN 1427:2015, IDT)) Bitumen and bituminous binders - Determinationof the softening point - Ring and Ball method]. Vid. ofіc. Kiїv: UkrnNDNC. 2019. 20 p. (Information and documentation). [in Ukrainian].
  30. DSTU B.V.2.7-81-98 Budіvelnі materіali. Bіtumi naftovі dorozhnі vyazkі. Metod viznachennja pokaznika zcheplennja z poverhneju skla ta kamjanih materіalіv (State  Standard of  Ukraine (DSTU B.V.2.7-81-98) Viscous road oil bitumens. The method to determine the index of engagement with the surface of glass and rock materials). Kyiv, 1999. 5 p. (Information and documentation) [in Ukrainian].
  31. Gun R.B. Neftjanye bitumy [Petroleum bitumen]. M.: Himija, 1973. 432 p. [in Russian].
  32. Glover C. J. et al. Development of a new method for assessing asphalt binder durability with field validation. Texas Dept Transport. 2005. Т. 1872. Р. 1–334 [in English].
  33. Bahia H.U. et al. Characterization of modified asphalt binders in Superpave mix design. Transportation Research Board, NCHRP report 459. 2001. 53 р. [in English].
  34. DSTU 8825:2019 Bіtum ta bіtumnі vyazhuchі. Metod viznachennja roztjazhnostі. [State  Standard of  Ukraine (DSTU 8825:2019) Bitumen and bituminous. Stretching method]. Kyiv, 2020. 9 p. (Information and documentation) [in Ukrainian].